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The approach developed for the synthesis of the pyrrolidine-containing Ugi product **31** is also applicable for the analogous synthesis of the propane derivative **32** ([Scheme 13](#C13){ref-type=”fig”}).
{#C13}
Conclusion
==========
In conclusion, we have described a concise Ugi four-component condensation of 2-bromobenzaldehydes, propiolamide, *o*-nitrobenzaldehyde, and aldehyde as a key step of an efficient preparation of biologically relevant 1,3,5-trisubstituted pyrrolidines. The relative instability of some substrates in this reaction has been taken into consideration. A wide range of *o*-phenylenediamines and 1,3-diamines were shown to be suitable catalysts for the formation of *o*-phenylenediamine-substituted Ugi adducts, which have not been previously observed. Moreover, the new Ugi-carbamates were efficiently formed by the reaction of dicarbonyl compounds, *o*-phenylenediamines, and aminoketones. The use of dicarbonyl compounds, in particular, constituted a significant advantage of the proposed approach, especially in comparison to the existing Ugi-amides and Ugi–phenol condensations. Moreover, the synthesis of propane-containing Ugi adducts is described.
Supporting Information
======================
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